Synthesis and Characterization of Carbon Soot Particles Doped HPMC Polymer Composites
DOI:
https://doi.org/10.6000/1929-5995.2015.04.02.1Keywords:
HPMC, Carbon Soot, XRD, Crystallite SizeAbstract
Biodegradable Hydroxyl propyl Methyl cellulose based polymer composites of various concentrations were prepared by doping carbon particles of kerosene soot. These composites were synthesized by employing simple solution casting method, to study the physical properties of the same. The analytical studies like XRD, AC conductivity, Tensile strength, Acoustic impedance, AFM and FTIR spectroscopy were carried out to characterize these composites. From the results it is seen that, the amorphous carbon particle disturbs the semi crystalline nature of the polymer by getting interstitial into polymer network. Further, this results in the characteristic changes of other physical parameters like tensile strength and AC conductivity. We have made an attempt to establish a structure property relation of such changes in the physical properties with that of microstructural parameters derived from XRD.
References
Siepmann J, Peppas NA. Modelling of drug release from delivery systems based on hydroxypropyl methylcellulose (HPMC). Adv Drug Deliv Rev 2001; 48: 139-57. http://dx.doi.org/10.1016/S0169-409X(01)00112-0
Phaechamud T. Variables Influencing Drug release from layered matrix system comprising Hydroxypropyl Methylcellulose. AAPS Pharm Sci Tech 2008. http://dx.doi.org/10.1208/s12249-008-9085-1
Talukdar MM, Michoel A, Rombout P, Kinget R. Comparative study on Xanthan gum and Hydroxypropyl methyl cellulose as matrices for controlled drug delivery. I.Compaction and In vitro drug release behaviour. Int J Pharm1996; 129: 233-41.
Ntaote David Shooto, Ezekiel Dixon Dikio. Synthesis and characterization of Diesel, Kerosene and Candle wax soot’s. Int J Electrochem Sci 2012; 7: 4335-44.
Tawansi A, Zidan HM, Oraby AH, Dorgham ME. Short-range-order spin clusters in one-dimensional Ising-like antiferromagnetic CoBr2-filled PVA films: a study of physical properties. J Phys D: Appl Phys 1998. http://dx.doi.org/10.1088/0022-3727/31/24/005
Davenas J, Xu XL, Boiteux G, Sage D. Relation between structure and electronic properties of ion irradiated polymers. Nucl Instr Meth B 1989; 39: 754-63. http://dx.doi.org/10.1016/0168-583X(89)90891-4
Williamson GK, Hall WH. X-Ray line broadening from filed aluminium and wolform. Acta Mettalurgica 1953; 1: 22-31. http://dx.doi.org/10.1016/0001-6160(53)90006-6
Urs TGK, Dasaiah M, Somashekar R. Studies on structural and conducting properties of goethite nanoparticles doped HPMC polymer films. J Polym 2014. http://dx.doi.org/10.1155/2014/201464
Aruldhas G. Molecular Structure and Spectroscopy, 2nd ed Prentice-Hall of India, New Delhi, 2004.
Sangappa AS, Demappa T, Sanjeev G, Parameswara P, Somashekar R. Spectroscopic and thermal studies of 8MeV electron beam irradiated HPMC films. 2009; 267: 2385-9.
Bajram Z, Janine A. Couplants and their influence on AE sensor sensitivity Pete Theobald, National Physical Laboratory. J Acoustic Emission 2008; 26: 91-7.
Guofeng B, Fusheng S, Jun Y, Chengguang Z. Elastic wave scattering by periodic cavities in backing material for ultrasound transducers. Available from http://medyna2013. sciencesconf.org/13237/document.
Yujie H, Robert CS, Keith NJ, Linda S. Schadler Rensselaer Some mechanistic understanding of the impulse strength of nanocomposites. Available from http://homepages.rpi.edu/ ~nelsoj/CEIDP2006_4.doc.
Soundappan T, Rong FY, Shen-Ming C. Palladium particles based nano films electrochemical fabrication, characterization and applications. Int J Electrochem Sci 2011; 6: 4537-52.
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2015 G.K. Gowtham, Vinayakprasanna N. Hegde, Simin Meshk, S.K. Sukrutha, R. Somashekar
This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.
Policy for Journals/Articles with Open Access
Authors who publish with this journal agree to the following terms:
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.
- Authors are permitted and encouraged to post links to their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work
Policy for Journals / Manuscript with Paid Access
Authors who publish with this journal agree to the following terms:
- Publisher retain copyright .
- Authors are permitted and encouraged to post links to their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work .